烯啶蟲胺是一類重要的煙堿類殺蟲劑中的新品種,具有高效、廣譜、低毒、耐抗性等特點(diǎn),在世界范圍內(nèi)得到了廣泛的應(yīng)用，是重要的糧食作物、經(jīng)濟(jì)作物等多種蟲害的優(yōu)良防治用藥。對(duì)于國(guó)內(nèi)現(xiàn)有的殺蟲劑難以防除的一些蟲害，特別是蚜蟲、葉蟬、半翅目害蟲、水稻飛虱等，顯示了卓越的活性，且防治費(fèi)用低廉。烯啶蟲胺低毒和對(duì)靶標(biāo)蟲害的特效作用也在獸藥方面得到了廣泛應(yīng)用。在世界范圍內(nèi)(包括中國(guó)在內(nèi))得到了的應(yīng)用，前景廣闊。
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1、1-二氯乙烯與鹽酸、硝酸反應(yīng)生成1、1、1-三氯-2-硝基乙烷，結(jié)束后需要加堿水中和，消除一分子氯化氫，生成1,1-二氯-2-硝基乙烯中間體，
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反應(yīng)生成1、1、1-三氯-2-硝基乙烷的收率僅能達(dá)到68％～80％
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浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司，研發(fā)氣相色譜法測(cè)定1,1,1-三氯-2-硝基乙烷的含量，面積歸一法定量，結(jié)果滿意。
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名稱：毛細(xì)管柱
固定相：專用
規(guī)格：30m*0.32mm*0.5um
型號(hào)：HH-CLNO2
溫度：240°C
應(yīng)用：
1.? ? ? 1,1-二氯-2-硝基乙烯測(cè)定分離
2.? ? ? 1、1、1-三氯-2-硝基乙烷的測(cè)定
3.? ? ??1,1-二氯-2-硝基乙烯的檢測(cè)
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Fenpropathrin is an important new variety of nicotine insecticides, characterized by high efficiency, broad-spectrum, low toxicity, and resistance. It has been widely used worldwide and is an excellent control drug for various pests such as important food crops and cash crops. For some pests that are difficult to control with existing insecticides in China, especially aphids, leafhoppers, hemiptera pests, rice planthoppers, etc., they have shown excellent activity and low control costs. The low toxicity and specific effects on target pests of enacloprid have also been widely used in veterinary medicine. It has been applied worldwide (including China) and has broad prospects.
1. 1-Dichloroethylene reacts with hydrochloric acid and nitric acid to produce 1,1,1-trichloro-2-nitroethane. After completion, alkaline water needs to be added to eliminate one molecule of hydrogen chloride and generate an intermediate of 1,1-dichloro-2-nitroethylene,
The yield of 1,1,1-trichloro-2-nitroethane generated by the reaction can only reach 68% to 80%
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has developed a gas chromatography method to determine the content of 1,1,1-trichloro-2-nitroethane, and the area normalization method has been used for quantification, with satisfactory results.
Name: Capillary Column
Fixed phase: dedicated
Specification: 30m * 0.32mm * 0.5um
Model: HH-CLNO2
Temperature: 240 ° C
Application:
1. Determination and separation of 1,1-dichloro-2-nitroethylene
Determination of 1,1,1-trichloro-2-nitroethane
3. Detection of 1,1-dichloro-2-nitroethylene
滕州市浩瀚色譜儀器技術(shù)服務(wù)有限公司
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