藥典二氧化碳中指標(biāo)要求：
碳?xì)浠衔镎諝庀嗌V法(通則0521)測(cè)定供試品氣體取本品,即得對(duì)照品氣體取甲烷含量為0.0020%的氣體(以氮?dú)鉃橄♂寗?。色譜條件用玻璃球?yàn)樘盍系纳V柱(4mm×0.8m,80目);柱溫為110℃;進(jìn)樣口溫度為110℃;檢測(cè)器為火焰離子化檢測(cè)器,溫度為120℃測(cè)定法精密量取供試品氣體與對(duì)照品氣體,分別注入氣相色譜儀,在凈化溫度為360℃時(shí)測(cè)得的峰面積為相應(yīng)空白值;精密量取供試品氣體與對(duì)照品氣體,分別注入氣相色譜儀,測(cè)定峰面積,減去相應(yīng)空白值后的峰面積為校正峰面積限度按外標(biāo)法以校正峰面積計(jì)算,含碳?xì)浠衔?以甲烷計(jì))不得過(guò)0.0020%。
名稱(chēng)：玻璃球填充柱
規(guī)格：0.8m*4mm，80目
最高使用溫度：300°C
編號(hào)：20230504001
應(yīng)用：中國(guó)藥典二氧化碳2020年版
適用于安捷倫7890,6890,7820A，8860,8890
浩瀚色譜研制生產(chǎn)的玻璃球柱，效果良好，滿(mǎn)足藥典二氧化碳的分析要求。浩瀚色譜，提供詳細(xì)的分析方法。
Pharmacopoeia Carbon Dioxide Index Requirements:
Hydrocarbons are measured using gas chromatography (General Rule 0521) to obtain the reference gas, which is a gas with a methane content of 0.0020% (using nitrogen as the diluent). Chromatographic conditions: Chromatographic column filled with glass balls (4mm × 0.8m, 80 mesh); The column temperature is 110 ℃; The inlet temperature is 110 ℃; The detector is a flame ionization detector, with a temperature of 120 ℃. The test gas and reference gas are accurately measured and injected into a gas chromatograph. The peak area measured at a purification temperature of 360 ℃ is the corresponding blank value; Accurately measure the test sample gas and the control sample gas, inject them into a gas chromatograph, measure the peak area, subtract the corresponding blank value, and the peak area is the corrected peak area limit. Calculate the corrected peak area using the external standard method, and the hydrocarbon content (calculated as methane) shall not exceed 0.0020%.
Name: Glass ball filled column
Specification: 0.8m * 4mm, 80 mesh
Maximum operating temperature: 300 ° C
No.: 20230504001
Application: Chinese Pharmacopoeia Carbon Dioxide 2020 Edition
Applicable to Agilent 789068907820A, 88608890
The glass ball column developed and produced by Haohan Chromatography has good results and meets the analysis requirements of carbon dioxide in the Pharmacopoeia. Vast chromatography, providing detailed analysis methods.
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