麝香(musk)是雄性鹿科動物香囊中的分泌物,是一種極其珍貴的香料,早在東漢時期麝香就被稱作香料之王。通常香精中只要加入萬分之一的麝香,就能使香氣變得柔和誘人且經(jīng)久不散,因而它是高檔香精中不可缺少的定香劑。
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浩瀚色譜(山東)應(yīng)用技術(shù)開發(fā)有限公司,采用氣相色譜法測定麝香酮藥效成分含量的方法。,提取準(zhǔn)確度平均回收率為101.64%,RSD為3.67%;線性方程為y=2394.6x+600.7,相關(guān)系數(shù)r=0.99995表明范圍在1.0~100.0μg/m L范圍內(nèi)線性關(guān)系良好。從氣相色譜結(jié)果中顯示,自制方法比藥典方法專屬性更好,樣品基線分離更優(yōu)越,更適合。
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名稱:填充柱
固定相:50%苯基-甲基聚硅氧烷
規(guī)格:2m*3mm
型號:2%OV-17/CWA
應(yīng)用:藥典麝香酮分析
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Musk is the secretion from the sachet of male deer and is an extremely precious spice. As early as the Eastern Han Dynasty, Musk was known as the king of spices. Generally, as long as 1/10000 musk is added to essence, the fragrance will become soft, attractive and lasting. Therefore, it is an indispensable fragrance fixative in high-end essence.
Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. uses gas chromatography to determine the content of active ingredients in muscone., The average recovery rate of extraction accuracy is 101.64%, and the RSD is 3.67%; The linear equation is y=2394.6x+600.7, and the correlation coefficient r=0.99995 indicates a good linear relationship within the range of 1.0~100.0 μ g/mL. The gas chromatography results show that the self-made method has better specificity than the pharmacopoeia method, and the sample baseline separation is superior and more suitable.
Name: Filler Column
Fixed phase: 50% phenyl methyl polysiloxane
Specification: 2m * 3mm
Model: 2% OV-17/CWA
Application: Pharmacopeia Musk Ketone Analysis
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