聚丙烯裝置生產(chǎn)中對(duì)丙烯原料中一氧化碳、二氧化碳含量控制較為嚴(yán)格,特別是使用茂金屬催化劑后,對(duì)丙烯中的一氧化碳、二氧化碳含量要求提升到uL/m~3級(jí),而目前所用的分析方法GB/T 3394-2009《工業(yè)用乙烯、丙烯中微量一氧化碳、二氧化碳和乙炔的測(cè)定氣相色譜法》最低檢出限只能達(dá)到mL/m~3級(jí),完全不能適應(yīng)目前更高的要求;
浩瀚色譜(山東)應(yīng)用技術(shù)開(kāi)發(fā)有限公司通過(guò)對(duì)分析方法實(shí)驗(yàn)條件的改造優(yōu)化,以及試驗(yàn)摸索,建立了可檢測(cè)丙烯中微量一氧化碳、二氧化碳分析方法,結(jié)果表明:經(jīng)優(yōu)化后的方法測(cè)定丙烯中一氧化碳與二氧化碳最低檢出限分別可達(dá)5uL/m~3與18uL/m~3,方法3次重復(fù)測(cè)定被測(cè)組分的相對(duì)標(biāo)準(zhǔn)偏差均小于12.85%,數(shù)據(jù)的精密度良好,可滿足聚丙烯裝置試用茂金屬催化劑對(duì)丙烯檢測(cè)的技術(shù)要求。
HH-790CH4-GC甲烷轉(zhuǎn)化爐的轉(zhuǎn)化效率gao,安裝簡(jiǎn)單,便攜式,小巧玲瓏,集成加熱,氣路,進(jìn)樣,溫控,柱分離系統(tǒng)于一體;可擴(kuò)展為二維/多維,反吹,切割系統(tǒng)。
名稱:便攜式甲烷轉(zhuǎn)化爐
型號(hào):HH-790CH4-GC
應(yīng)用: GB/T 3394-2009工業(yè)用乙烯、丙烯中微量一氧化碳、二氧化碳和乙炔的測(cè)定 氣相色譜法
適合于:安捷倫4890. 5890, 6890, 7890, 7820, 8860, 8890氣相色譜儀上
The content of carbon monoxide and carbon dioxide in propylene feedstock is strictly controlled in the production of polypropylene plant, especially after the use of metallocene catalyst, the requirement for carbon monoxide and carbon dioxide in propylene is raised to the level of uL/m~3, while the minimum detection limit of the currently used analytical method GB/T 3394-2009 "Determination of trace carbon monoxide, carbon dioxide and acetylene in ethylene and propylene for industrial use by gas chromatography" can only reach the level of mL/m~3, It is completely unable to meet the current higher requirements;
Haohan Chromatography (Shandong) Applied Technology Development Co., Ltd. has established an analytical method that can detect trace carbon monoxide and carbon dioxide in propylene through the transformation and optimization of the experimental conditions of the analytical method and experimental exploration. The results show that the minimum detection limit of carbon monoxide and carbon dioxide in propylene can reach 5uL/m3 and 18uL/m3 respectively by the optimized method, and the relative standard deviation of the three repeated determinations of the tested components is less than 12.85%, The precision of the data is good, which can meet the technical requirements for propylene detection by using metallocene catalyst in polypropylene plant.
The conversion efficiency of HH-790CH4-GC methane conversion furnace is gao, which is simple to install, portable, small and exquisite, and integrates heating, gas path, sample injection, temperature control, and column separation system; It can be extended to 2D/multi-dimension, blowback and cutting systems.
Name: portable methane converter
Model: HH-790CH4-GC
Application: GB/T 3394-2009 Determination of trace carbon monoxide, carbon dioxide and acetylene in ethylene and propylene for industrial use Gas chromatography
Applicable to: Agilent 4890. 5890, 6890, 7890, 7820, 8860, 8890 gas chromatograph
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